Handbook of Sample Preparation (eBook)

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2012
John Wiley & Sons (Verlag)
978-0-470-88019-7 (ISBN)

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Discover new keys to solving analytical problems using the Latest sample preparation methods Commonly viewed of as a routine task rather than as an integral component in the analytical process, sample preparation has long been undervalued as a science and underdeveloped as a technology. In an effort to reverse this trend, Handbook of Sample Preparation shows why sample preparation deserves closer scientific scrutiny, and makes a compelling case for colleges and professional laboratories to devote more resources to promote the benefits of its correct application. Handbook of Sample Preparation includes: A solid overview of standard sampling methodologies and their analytical capabilities An introduction of non-traditional sampling technologies, which address the need for solvent-free alternatives, automation, and miniaturization A discussion of the analytical shift toward performing sampling on-site, rather than in the laboratory An examination of various extraction technologies and their applications for different types of matrices A look at how to take advantage of new sampling strategies to streamline laboratory procedures, reduce research costs, and increase overall productivity An excellent primer on the fundamentals of extraction as well as a sound guide on the latest technological upgrades influencing current sampling techniques, this versatile text serves as an important and accessible tool for both students and seasoned practitioners as they seek new avenues for improving the accuracy of their analyses.

JANUSZ PAWLISZYN, PhD, is a Professor in the Department of Chemistry at the University of Waterloo in Ontario, Canada. He is the author of Solid Phase Microextraction (Wiley) and Sampling and Sample Preparation in Field and Laboratory, and has been published in more than four hundred scientific publications. HEATHER L. LORD, PhD, is a Research Associate for New Analytical Methods and Technologies in the Department of Chemistry at the University of Waterloo. She received her PhD in 2005 under Dr. Pawliszyn.

Preface.

Contributors.

Part I Fundamental Extraction Techniques.

1 Theory of Extraction (Janusz Pawliszyn).

2 Headspace Gas Chromatography (Zelda E. Penton).

3 Liquid-Liquid Extraction in Environmental Analysis
(Toh Ming Hii and Hian Kee Lee).

4 Solid-Phase Extraction (Ronald E. Majors).

5 Solid-Phase Microextraction (Sanja Risticevic, Dajana
Vuckovic, and Janusz Pawliszyn).

6 Microdialysis Sampling as a Sample Preparation Method
(Pradyot Nandi and Susan M. Lunte).

7 Liquid-Phase Microextraction (LPME) Utilizing Porous Hollow
Fibers (Stig Pedersen-Bjergaard, Knut Einar Rasmussen, and Jan
Åke Jönsson).

8 Sample Preparation in Membrane Introduction Mass Spectrometry
(Raimo A. Ketola, Tapio Kotiaho, and Frants R.
Lauritsen).

9 Pressurized Fluid Extraction (John R. Dean and Renli
Ma).

10 Superheated Water Extraction (Roger M. Smith).

11 Supercritical Fluid Extraction (Jeremy J. Kroon and
Douglas E. Raynie).

12 Microwave-Assisted Extraction (J.R. Jocelyn Paré and
Jacqueline M.R. Bélanger).

13 Chemical Derivatizations in Analytical Extractions (Jack
Rosenfeld).

Part II Application Considerations.

14 Sample Preparation Techniques for Environmental Organic
Pollutant Analysis (Ray E. Clement and Chunyan Hao).

15 Sample Preparation for the Study of Flavor Compounds in Food
(Henryk H. Jelen).

16 Sampling and Sample Preparation for Clinical and
Pharmaceutical Analysis (Hiroyuki Kataoka, Keita Saito, and
Atsushi Yokoyama).

17 Statistics of Sampling and Sample Preparation (Byron
Kratochvil).

18 SPME Devices Integrating Sampling with Sample Preparation for
On-Site Analysis (Gangfeng Ouyang).

Part III Recent Developments.

19 Developments in the Use of Passive Sampling Devices for
Monitoring Pollutants in Water (Graham A. Mills, Rocio
Aguilar-Martínez, Richard Greenwood, Ian J. Allan, Janine
Brümmer, Jesper Knutsson, and Branislav Vrana).

20 Solid-Phase Microextraction for Drug Analysis (Heather L.
Lord).

21 Sample Handling Protocols for Biosensor Applications
(Andrew Chan, Teresa Artuso, and Ulrich J. Krull).

22 Sol-Gel Coatings and Monoliths in Analytical Sample
Preparation (Scott Segro and Abdul Malik).

23 The Use of Molecularly Imprinted Polymers for Sampling and
Sample Preparation (Börje Sellergren and Antonio Martin
Esteban).

Index.

"Handbook of Sample Preparation" is a valuable book
dealing with a wide range of state-of-the-art extraction techniques
that have been used in many laboratories. Not only a good text book
on a variety of extraction techniques, it also enables systematic
understanding of the modern sample-preparation methods necessary
for workers dealing with the analysis of various complex
mixtures." (Anal Bioanal Chem, 2011)

Erscheint lt. Verlag 16.5.2012
Sprache englisch
Themenwelt Naturwissenschaften Chemie Analytische Chemie
Technik
Schlagworte Analytical • Analytical Chemistry • Analytische Chemie • Biowissenschaften • CASE • Chemie • Chemistry • commonly • deserves closer • Discover • effort • Genomforschung u. Proteomik • Genomics & Proteomics • Handbook • Latest • Life Sciences • materials characterization • Materials Science • Materialwissenschaften • Methods • New • Preparation • Probenvorbereitung • Problems • Routine • Sample • sample preparation • Science • scientific scrutiny • Task • Technology • underdeveloped • undervalued • Werkstoffprüfung • Werkstoffprüfung
ISBN-10 0-470-88019-8 / 0470880198
ISBN-13 978-0-470-88019-7 / 9780470880197
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