Handbook of Sample Preparation

Janusz Pawliszyn, Heather L. Lord (Herausgeber)

Buch | Hardcover

512 Seiten

2010
Wiley-Blackwell (Verlag)
978-0-470-09934-6 (ISBN)

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* Provides a comprehensive reference for all of the most common sample preparation techniques and applications * Begins by providing a unified theory of extraction and goes on to discuss the fundamentals of extraction techniques, specific sample preparation techniques, recent developments, and sampling.

Discover new keys to solving analytical problems using the Latest sample preparation methods Commonly viewed of as a routine task rather than as an integral component in the analytical process, sample preparation has long been undervalued as a science and underdeveloped as a technology. In an effort to reverse this trend, Handbook of Sample Preparation shows why sample preparation deserves closer scientific scrutiny, and makes a compelling case for colleges and professional laboratories to devote more resources to promote the benefits of its correct application.

Handbook of Sample Preparation includes:

A solid overview of standard sampling methodologies and their analytical capabilities
An introduction of non-traditional sampling technologies, which address the need for solvent-free alternatives, automation, and miniaturization
A discussion of the analytical shift toward performing sampling on-site, rather than in the laboratory
An examination of various extraction technologies and their applications for different types of matrices
A look at how to take advantage of new sampling strategies to streamline laboratory procedures, reduce research costs, and increase overall productivity

An excellent primer on the fundamentals of extraction as well as a sound guide on the latest technological upgrades influencing current sampling techniques, this versatile text serves as an important and accessible tool for both students and seasoned practitioners as they seek new avenues for improving the accuracy of their analyses.

JANUSZ PAWLISZYN, PhD, is a Professor in the Department of Chemistry at the University of Waterloo in Ontario, Canada. He is the author of Solid Phase Microextraction (Wiley) and Sampling and Sample Preparation in Field and Laboratory, and has been published in more than four hundred scientific publications. HEATHER L. LORD, PhD, is a Research Associate for New Analytical Methods and Technologies in the Department of Chemistry at the University of Waterloo. She received her PhD in 2005 under Dr. Pawliszyn.

Preface vii

Contributors ix

Part I Fundamental Extraction Techniques 1

1 Theory of Extraction 3
Janusz Pawliszyn

2 Headspace Gas Chromatography 25
Zelda E. Penton

3 Liquid–Liquid Extraction in Environmental Analysis 39
Toh Ming Hii and Hian Kee Lee

4 Solid-Phase Extraction 53
Ronald E. Majors

5 Solid-Phase Microextraction 81
Sanja Risticevic, Dajana Vuckovic, and Janusz Pawliszyn

6 Microdialysis Sampling as a Sample Preparation Method 103
Pradyot Nandi and Susan M. Lunte

7 Liquid-Phase Microextraction (LPME) Utilizing Porous Hollow Fibers 125
Stig Pedersen-Bjergaard, Knut Einar Rasmussen, and Jan Åke Jönsson

8 Sample Preparation in Membrane Introduction Mass Spectrometry 149
Raimo A. Ketola, Tapio Kotiaho, and Frants R. Lauritsen

9 Pressurized Fluid Extraction 163
John R. Dean and Renli Ma

10 Superheated Water Extraction 181
Roger M. Smith

11 Supercritical Fluid Extraction 191
Jeremy J. Kroon and Douglas E. Raynie

12 Microwave-Assisted Extraction 197
J.R. Jocelyn Paré and Jacqueline M.R. Bélanger

13 Chemical Derivatizations in Analytical Extractions 225
Jack Rosenfeld

Part II Application Considerations 247

14 Sample Preparation Techniques for Environmental Organic Pollutant Analysis 249
Ray E. Clement and Chunyan Hao

15 Sample Preparation for the Study of Flavor Compounds in Food 267
Henryk H. Jeleń

16 Sampling and Sample Preparation for Clinical and Pharmaceutical Analysis 285
Hiroyuki Kataoka, Keita Saito, and Atsushi Yokoyama

17 Statistics of Sampling and Sample Preparation 313
Byron Kratochvil

18 SPME Devices Integrating Sampling with Sample Preparation for On-Site Analysis 325
Gangfeng Ouyang

Part III Recent Developments 341

19 Developments in the Use of Passive Sampling Devices for Monitoring Pollutants in Water 343
Graham A. Mills, Rocio Aguilar-Martínez, Richard Greenwood, Ian J. Allan, Janine Brümmer, Jesper Knutsson, and Branislav Vrana

20 Solid-Phase Microextraction for Drug Analysis 365
Heather L. Lord

21 Sample Handling Protocols for Biosensor Applications 385
Andrew Chan, Teresa Artuso, and Ulrich J. Krull

22 Sol-Gel Coatings and Monoliths in Analytical Sample Preparation 419
Scott Segro and Abdul Malik

23 The Use of Molecularly Imprinted Polymers for Sampling and Sample Preparation 445
Börje Sellergren and Antonio Martin Esteban

Index 475

Erscheint lt. Verlag	9.11.2010
Verlagsort	Hoboken
Sprache	englisch
Maße	225 x 287 mm
Gewicht	1420 g
Themenwelt	Naturwissenschaften ► Chemie ► Analytische Chemie
ISBN-10	0-470-09934-8 / 0470099348
ISBN-13	978-0-470-09934-6 / 9780470099346
Zustand	Neuware