Inorganic Syntheses, Volume 11 (eBook)

William L. Jolly is the editor-in-chief of Inorganic Syntheses, Volume 11, published by Wiley.

Preface.

Notice to Contributors.

Chapter One THE SOLID STATE.

1. Barium and Strontium Molybdates(IV).

2. Cadmium Digallium(III) Tetrasulfide.

3. Single Crystals of Triiron Tetraoxide.

ChupterTwo BORON-HYDROGENCOMPOUNDS.

4. Diborane.

5. closo-1,2-Dicarbadodecaborane(l2)
[1,2-Dicarbaclovodode-caborane(12)].

6. Polyhedral Hydroborates.

7. C-Amminecarbaundecaborane(12) Derivatives and Cesium
Tridecahydrocarbaundecaborate(1-).

8. Transition-metal Complexes of
B10H10CNH3¯2- and
B10H10CH¯3-.

Chapter Three COORDINATION COMPOUNDS.

9. Lattice-stabilized Complex Ions.

10. Potassium Octacyanomolybdate(IV) 2-Hydrate.

11. Manganates(VI).

12. Bis(dimethylg1yoximato) cobalt Complexes
("Cobaloximes").

13. Potassium mu-Oxo-bis[pentachlororuthenate(IV)]
1-Hydrate.

14. Vanadium(III), Cobalt(II), and Nickel(II) beta-Keto Amine
Complexes.

15. Hexacoordinate Complexes of Bis(2,4-pentanedionato)
cobalt(II) [Bis(acetylacetonato) cobalt(II)].

16. Metal Derivatives of 2,2'-Iminobis(acetamidoxime).

17. Volatile Rare-earth Chelates of 2,2,6,6-Tetramethylheptaen
-3,5-dione.

18. trans-Chlorocarbonylbis (triphenylphosphine) rhodium
and Related Complexes.

19. trans-Chlorocarbonylbis (triphenylphosphine)
iridium.

20. Tris- and Tetrakis (triphenylphosphine) platinum(0).

21. Square Planar Dichloropalladium(II) Complexes with
Organophosphorus Ligands.

Chapter Four THE DEPROTONATION OF WEAK ACIDS WITH
POTASSIUM HYDROXIDE: APPLICATIONS TO THE SYNTHESIS OF
ORGANOMETALLICCOMPOUNDS.

22. sigma-Methyl-pi-cyclopentadienylmolybdenum
Tricarbonyl.

23. Bis(cyclopentadienyl) iron (Ferrocene).

24. Bis(cyclopentadienyl) nickel (Nickelocene).

25. Methylphosphine.

26. Dimethylphosphine.

27. Methylgermane.

Chapter Five FLUORINE COMPOUNDS.

28. Thionyl Tetrafluoride and Pentafluorosulfur
Hypofluorite.

29. Imidodisulfuryl Fluoride, Cesium Imidodisulfuryl Fluoride,
and Fluoroimidodisulfuryl Fluoride.

30. Bis(fluoroxy) difluoromethane.

31. Xenon Difluoride.

32. Disulfuryl Fluoride (Pyrosulfuryl Fluoride).

33. Peroxydisulfuryl Difluoride (A Note of Warning).

Chapter Six MISCELLANEOUS NONMETALLIC
COMPOUNDS.

34. Dimethylphosphine.

35. Bromosilane, Iodosilane, and Trisilylamine.

36. Silane, Stannane, Silane-d4,
Germane-d4, and
Stannane-d4.

37. Trialkoxyarsines (Trialkyl Arsenites).

38 . Sulfur Imides.

39. Nitrosyl Halides.

40. Trimeric Phenylphosphonitrile Bromides.

41. Xenon Trioxide Solution.

42. Sodium Perxenate (Sodium Xenate(VIII)).

Corrections.

Copper(I) Iodide.

Dichlorobis(4-chlorobutenyl) dipalladium(II).

Nitrogen Compounds.

Index of Contributors.

Subject Index.

Formula Index.