Chemistry: Inorganic Qualitative Analysis in the Laboratory

To the InstructorChapter 1 Introduction to Qualitative Analysis in the Laboratory 1.1 An Overview of Inorganic Qualitative Analysis 1.2 Definitions of Terms Used in Qualitative AnalysisChapter 2 Equipment, Reagents, and Procedures 2.1 The Semimicro Scale 2.2 Basic Glassware Cleaning Glassware Stirring Rods Droppers and Pipets Wash Bottles 2.3 Reagents 2.4 Handling Solutions and Reagents Measuring and Transferring Solutions and Reagents Diluting and Mixing Solutions and Reagents Heating Solutions Evaporating Solutions Testing Solutions 2.5 Handling Precipitates Precipitation Separating Precipitates by Centrifugation Washing and Transferring Precipitates after Centrifugation Separating Precipitates by Filtration Washing and Transferring Precipitates after Filtration Sulfide Precipitations 2.6 Flame Tests 2.7 Laboratory Safety General Safety Precautions Avoiding Burns Avoiding Cuts Avoiding Chemical AccidentsChapter 3 Laboratory Records and Preliminary Experiments 3.1 Making and Recording Observations 3.2 The Laboratory Notebook 3.3 The Laboratory Report 3.4 Preliminary Experiments Experiment 1. Classification of Precipitates Experiment 2. Handling Precipitates Experiment 3. Separation Techniques Experiment 4. Flame Tests Experiment 5. Volatization Experiment 6. Brown Ring Test Experiment 7. Solvent Extraction Prelaboratory Questions Laboratory ReportChapter 4 Preparations for Anion and Cation Analysis 4.1 Reading the Written Procedures 4.2 Preparing a Sample for Anion or Cation Analysis General Solubility Considerations Samples for Anion Analysis Samples for Cation Analysis Dissolution of AlloysChapter 5 Qualitative Analysis for Anions 5.1 Anions: The Preliminary Tests 5.2 Anions: The Specific Tests Prelaboratory Questions Laboratory ReportChapter 6 Qualitative Analysis for Cations 6.1 Procedures for Analysis of Cation Group 1 Prelaboratory Questions Laboratory Report 6.2 Procedures for Analysis of Cation Group II Prelaboratory Questions Laboratory Report 6.3 Procedures for Analysis of Cation Group III Prelaboratory Questions Laboratory Report 6.4 Procedures for Analysis of Cation Group IV Prelaboratory Questions Laboratory Report 6.5 Procedures for Analysis of Cation Group V Prelaboratory Questions Laboratory Report Laboratory Reports for Unknowns and Alloy AnalysisAppendix List of Equipment