Handbook of Environmental Analysis

Analytical Techniques
Introduction
Precision and Accuracy of Analysis
Analysis of Organic Pollutants by Gas Chromatography
Analysis of Organic Pollutants by Gas Chromatography/Mass Spectrometry
Extraction of Organic Pollutants and Sample Cleanup
Titrimetric Analysis
Colorimetric Analysis
Analysis of Metals by Atomic Absorption and Emission Spectroscopy
Ion-Selective Electrode Analysis
Application of High Performance Liquid Chromatography in Environmental Analysis
Ion Chromatography
Air Analysis
Application of Immunoassay Techniques in Environmental Analysis
Specific Classes of Substances and Aggregate Properties
Aldehydes and Ketones
Alkalinity
Bromide
Chloride
Cyanate
Cyanide, Total
Cyanide Amenable to Chlorination
Fluoride
Halogenated Hydrocarbons
Hardness
Herbicides: Chlorophenoxy Acid
Hydrocarbons
Hydrocarbons, Polynuclear Aromatic
Nitrogen (Ammonia)
Nitrogen (Nitrate)
Nitrosamines
Oxygen Demand, Biochemical
Oxygen Demand, Chemical
Pesticides: Carbamate, Urea and Triazine
Pesticides: Organochlorine
Pesticides: Organophosphorus
pH and Eh
Phenols
Phosphorus
Phthalate Esters
Polychlorinated Biphenyls (PCBs)
Polychlorinated Dioxins and Dibenzofurans
Silica
Sulfate
Sulfide
Sulfite
Surfactant: Anionic
Thiocyanate
Selected Individual Compounds
Acetaldehyde
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Aniline
Arsine
Asbestos
Benzene
Benzidine
Benzyl chloride
1,3-Butadiene
Carbon Disulfide
Carbon Monoxide
Carbon Tetrachloride
Captan
Chloroacetic acid
Chlorobenzene
Chloroform
2-Chlorophenol
Cumene
Cyanogen
Cyanuric Acid
Diazomethane
Diborane
Dichlorobenzene
1,1-Dichlorethylene
2,4-Dichlorophenol
Diethyl Ether
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Epichlorohydrin
Ethyl Chloride
Ethylene Chlorohydrin
Ethylene Dibromide
Ethylene Glycol
Ethylene Oxide
Formaldehyde
Freon-113
Hydrogen Cyanide
Hydrogen Sulfide
Isophorone
Methane
Methyl Bromide
Methyl Chloride
Methylene Chloride
Methyl Isobutyl Ketone
Methyl Isocyanate
Methyl Methacrylate
Nitrobenzene
Nitrogen Dioxide
Pentachlorophenol
Phosgene
Pyridine
Pyrocatechol
Pyrogallol
Resorcinol
Stibine
Strychnine
Styrene
Sulfur Dioxide
Tetrachloroethylene
Tetraethyllead
Tetraethyl Pyrophosphate
Tetrahydrofuran
Toluene
Toluene-2,4-Diisocyanate
o-Toluidine
1,1,1-Trichloroethane
Trichloroethylene
2,4,6-Trichlorophenol
Vinylchloride
Xylene
Appendices
Appendix A: Some Common QC Formulas and Statistics
Appendix B: Sample Containers, Preservations, and Holding Times
Appendix C: Preparation of Molar and Normal Solutions of Some Common Reagents
Appendix D: Total Dissolved Solids and Specific Conductance: Theoretical Calculations
Appendix E: Characteristic Masses for Identification of Additional Organic Pollutants (Not Listed in the Text) by GC/MS
Appendix F: Volatility of Some Additional Organic Substances (Not Listed in Text) for Purge and Trap Analysis
Appendix G: Analysis of Elements by Atomic Spectroscopy: An Overview
Appendix H: Analysis of Trace Elements by Inductively Coupled Plasma Mass Spectrometry
Appendix I: Oil and Grease Analysis: An Overview
Appendix J: NIOSH Methods for Air Analysis
Appendix K: U.S. EPA Methods for Air Analysis
Appendix L: Inorganic Test Procedures for Analysis of Aqueous Samples: EPA, SM, and ASTM Reference Methods
Appendix M: U.S. EPA Analytical Methods for Organic Pollutants in Aqueous and Solid Matrices
Indices
Chemical Compounds
CAS Registry Numbers