Gas Chromatography and Mass Spectrometry - Fulton G. Kitson, Barbara S. Larsen, Charles N. McEwen

Gas Chromatography and Mass Spectrometry

A Practical Guide
Buch | Softcover
381 Seiten
1996
Academic Press Inc (Verlag)
978-0-12-483385-2 (ISBN)
93,50 inkl. MwSt
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Provides information designed to facilitate the effectiveness of the GC/MS user. This guide contains a section on how to interpret mass spectral data, correlation of ion masses and neutral losses with possible structures, and examples of mass spectra. It includes information on instrumentation, ionization methods, and troubleshooting techniques.
This guide provides, under one cover, a wealth of practical information designed to facilitate the effectiveness of the GC/MS user. Separation conditions for numerous compound types are provided along with derivatized and underivatized compounds. A section on how to interpret mass spectral data, an extensive correlation of ion masses and neutral losses with possible structures, and examples of mass spectra are provided to further aid structure determination. Also included are basic information on instrumentation, ionization methods, quantitation, tips on the operation of mass spectrometers, the best derivatization procedures for a variety of compound types, troubleshooting techniques, and a variety of other information found to be useful to the practicing user of GC/MS instrumentation. This guide would be immediately valuable to the novice as well as the experienced GC/MS user who may not have the breadth of experience covered in this book. It condenses and organizes recent and essential information for new and experienced GC/MS users. It is comprehensively indexed and referenced. It includes practical methods of analysis.
It serves as a text reference for short practical courses on the subject.

Preface. Part I: The Fundamentals of GC/MS: What Is GC/MS. Mass Spectral Interpretation. Quantitation. Additional Literature Pertaining to Part I. Part II: GC Conditions, Derivatization, and Mass Spectral Interpretation of Specific Compound Types: Acids. Alcohols. Aldehydes. Amides. Amines. Amino Acids. Common Contaminants. Drugs and Metabolites. Esters. Ethers. Fluorinated Compounds. Gases. Glycols. Halogenated Compounds. Hydrocarbons. Isocyanates. Ketones. Nitriles. Nitroaromatics. Nitrogen-Containing Hetrocyclics. Nucleosides. Pesticides. Phenols. Phosphorus Compounds. Plasticizers. Prostaglandins. Solvents and Impurities. Steriods. Sugars. Sulfur Compounds. Additional Literature Pertaining to Part II. Part III: Ions for Determining Unknown Structures: M 1 to M 200. Part IV: Appendices: Definitions of Terms Related to Gas Chromatography. Tips for Gas Chromatography. Derivatives Found Useful in GC/MS. Cross Index Chart for GC Phases. McReynolds' Constants. Simple GC Troubleshooting. Definitions of Terms Related to Mass Spectrometry. Tips and Troubleshooting for Mass Spectrometry. Atomic Masses and Isotope Abundances. Structurally Significant McLafferty Rearrangement Ions. Isotope Patterns for ClxBry. Mixtures for Determining Mass Spectral Resolution. Additional Literature Pertaining to Part IV. Index.

Erscheint lt. Verlag 3.9.1996
Zusatzinfo index
Verlagsort San Diego
Sprache englisch
Maße 152 x 229 mm
Gewicht 538 g
Themenwelt Naturwissenschaften Chemie Analytische Chemie
ISBN-10 0-12-483385-3 / 0124833853
ISBN-13 978-0-12-483385-2 / 9780124833852
Zustand Neuware
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