Materials Syntheses -

Materials Syntheses

A Practical Guide
Buch | Softcover
VII, 228 Seiten
2010 | 1. Softcover reprint of hardcover 1st ed. 2008
Springer Wien (Verlag)
978-3-211-99912-7 (ISBN)
119,99 inkl. MwSt

Materials syntheses are generally more complex than syntheses of inorganic or organic compounds, and specific characterization methods play a more important role. Materials synthesis protocols often suffer from unclarities, irreproducibility, lack in detail and lack in standards. The need to change this situation is the main motivation for this book. A number of detailed protocols has been collected, ranging from organic polymers to carbonaceous and ceramic materials, from gels to porous and layered materials and from powders and nanoparticles to films. Preparation methods include intercalation and flux methods, sol-gel processing, templating methods for porous materials, sonochemistry or spray pyrolysis.

Each contribution provides detailed and unambiguous description of the hardware, specific characteristics of the procedure, scope of applicability as well as methods that unequivocally identify and characterize the material and allow checking whether the synthesis was successful.

Controlling Size and Morphology of Zeolite L.- Zeolite A and ZK-4.- Mesostructured Silica Thin Films.- Organically Modified Monolithic Silica Aerogels.- Porous Silica Gel by Acid Leaching of Metakaolin.- Zirconia-Pillared Clays.- Montmorillonites with Mixed Aluminum-Lanthanide Oxide Pillars.- Birnessite-type Manganese Oxide by Redox Precipitation.- Templated Carbon from Pyrolysis of Pyrene in Pillared Clay Matrices.- Fiberous Carbon from Sepiolite Clay and Propylene.- Aerosol Spray Synthesis of Porous Molybdenum Sulfide Powder.- Sonochemically Prepared Molybdenum Sulfide.- Doped Manganites.- Lithium Manganese Oxide Prepared by Flux Methods.- Nanoscale Magnesium Oxide.- Nanostructured Pt-doped Tin Oxide Films.- Organically Functionalized Silica Nanoparticles.- Copper Nanoparticles in Silica.- Copper Nanocrystals.- Assembly of TOPO-Capped Silver Nanoparticles to Multilayered Films.- Colloidal Dispersion of Gold Nanoparticles.- One-dimensional Nanorods and Nanowires.- Monolithic Tin-doped Silica Glass.- Octaphenyloctasilsesquioxane and Polyphenylsilsesquioxane for Nanocomposites.- Polysilsesquicarbodiimide Xerogels.- Polyaniline - A Conducting Polymer.- Allyl- and Hydroxytelechelic Poly(isobutylenes).- Symmetrically and Unsymmetrically Substituted Phthalocyanines.

Erscheint lt. Verlag 13.10.2010
Zusatzinfo VII, 228 p.
Verlagsort Vienna
Sprache englisch
Maße 155 x 235 mm
Gewicht 361 g
Themenwelt Naturwissenschaften Chemie Anorganische Chemie
Technik Maschinenbau
Schlagworte Aerogel • Chemistry • Inorganic Chemistry • Magnesium • Materials • Materials Chemistry • Materials Synthesis • nanostructure • Practical Guide • synthesis
ISBN-10 3-211-99912-4 / 3211999124
ISBN-13 978-3-211-99912-7 / 9783211999127
Zustand Neuware
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