Solid State NMR Studies of Biopolymers (eBook)

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2012 | 1. Auflage
592 Seiten
Wiley (Verlag)
978-1-118-58889-5 (ISBN)

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The content of this volume has been added to eMagRes (formerly Encyclopedia of Magnetic Resonance) - the ultimate online resource for NMR and MRI. The field of solid state NMR of biological samples [ssNMR] has blossomed in the past 5-10 years, and a cohesive overview of the technology is needed for new practitioners in industry and academia. This title provides an overview of Solid State NMR methods for studying structure dynamics and ligand-binding in biopolymers, and offers an overview of RF pulse sequences for various applications, including not only a systematic catalog but also a discussion of theoretical tools for analysis of pulse sequences. Practical examples of biochemical applications are included, along with a detailed discussion of the many aspects of sample preparation and handling that make spectroscopy on solid proteins successful. About EMR Handbooks / eMagRes Handbooks The Encyclopedia of Magnetic Resonance (up to 2012) and eMagRes (from 2013 onward) publish a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence of this large number of articles, written by experts in various fields, is enabling the publication of a series of EMR Handbooks / eMagRes Handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of articles from eMagRes. In consultation with the eMagRes Editorial Board, the EMR Handbooks / eMagRes Handbooks are coherently planned in advance by specially-selected Editors, and new articles are written (together with updates of some already existing articles) to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in academia or industry. Have the content of this Handbook and the complete content of eMagRes at your fingertips! Visit: www.wileyonlinelibrary.com/ref/eMagRes View other eMagRes publications here

Anne E. McDermott and Tatyana Polenova are the authors of Solid State NMR Studies of Biopolymers, published by Wiley.

Contributors.

Series Preface.

Volume Preface.

Part A: Fundamentals of Solid-State NMR Spectroscopy.

1 Internal Spin Interactions and Rotations in Solids (MichaelMehring).

2 Average Hamiltonian Theory (John S. Waugh).

3 Tensors inNMR (S. Chandra Shekar, Alexej Jerschow).

4 Chemical Shift Tensors (David M. Grant).

5 Magic Angle Spinning (E. Raymond Andrew).

6 Cross Polarization in Solids (Douglas P. Burum).

7 Quadrupolar Nuclei in Solids (Alexander J. Vega).

Part B: Recent Developments in Solid-State NMR Hardware andEmerging Methodologies for Structural and Dynamics Studies ofBiopolymers.

8 Probe Development for Biosolids NMR Spectroscopy (Peter L.Gor'kov, William W. Brey, Joanna R. Long).

9 High-Frequency Dynamic Nuclear Polarization (Melody L.Mak-Jurkauskas, Robert G. Griffin).

10 Homonuclear Dipolar Recoupling in Solid-State NMR (RobertTycko).

11 Dipolar Recoupling: Heteronuclear (Christopher P.Jaroniec).

12 Adiabatic Polarization-Transfer Methods in MAS Spectroscopy(Matthias Ernst, Beat H. Meier).

13 Symmetry-Based Pulse Sequences in Magic-Angle SpinningSolid-State NMR (Malcolm H. Levitt).

14 Dipolar-Based Torsion Angle Measurements for ProteinStructure Determination (Vladimir Ladizhansky).

15 Deuterated Peptides and Proteins: Structure and DynamicsStudies by MAS Solid-State NMR (Bernd Reif).

16 Correlation Spectroscopy for Resonance Assignments inSolid-State Proteins Using J-couplings (Leonard J. Mueller,Jeremy J. Titman).

17 Indirect Coupling and Connectivity (Anne Lesage).

18 Fast Magic-Angle Spinning for Protein Solid-State NMRSpectroscopy (Donghua H. Zhou).

19 Relaxation Studies of Solid Biopolymers (J´ozef R.Lewandowski, Lyndon Emsley).

Part C: Computational Aspects of Solid-State NMRSpectroscopy.

20 Proteins and Model Systems: Spectral Analyses (EricOldfield).

21 Numerical Simulations in Solid-State NMR with SIMPSON(Thomas Vosegaard, Zdencaronek Tocaronsner, Niels Chr.Nielsen).

22 Protein Structure Calculation Using Ambiguous Restraints(Michael Nilges, Th´er`ese Malliavin, BenjaminBardiaux).

23 Protein Structure Calculation and Automated NOE Restraints(Torsten Herrmann).

Part D: Applications of Solid-State NMR to Structural andDynamics Studies of Biopolymers.

24 Aligned Membrane Proteins: Structural Studies (Riqiang Fu,William W. Brey, Timothy A. Cross).

25 Membrane-Associated Systems: Structural Studies by MAS NMR(Christian Ader, Marc Baldus, Stefan Becker).

26 Structural Studies of Protein Fibrils and Misfolded Proteinsby Solid-State NMR (Beat H. Meier).

27 Structural and Dynamics Studies of Lipids by Solid-State NMR(Michele Auger).

28 REDOR Applications in Biology: An Overview (Orsolya Toke,Lynette Cegelski).

29 Quadrupolar Metal Nuclides in Bioinorganic Chemistry:Solid-State NMR Studies (Andrew S. Lipton, Tatyana Polenova,Paul D. Ellis).

30 Photosynthetic Antennae and Reaction Centers (Huub J. M.de Groot).

31 Structure and Function Studies of Energy and SignalTransducing Proteins by Solid-State NMR (Hideo Akutsu,Toshimichi Fujiwara).

32 Protein-Solvent Interactions in Solids (AnjaB¨ockmann).

33 Unifying Solution and Solid-State NMR Studies of Nucleic AcidDynamics (Kari Pederson, Dorothy C. Echodu, Prashant Emani, GregL. Olsen, Michael F. Bardaro Jr., Zahra Shajani, Gary A. Meints,Paul A. Miller, Gabriele Varani, Gary P. Drobny).

Index.

Erscheint lt. Verlag 19.12.2012
Sprache englisch
Themenwelt Naturwissenschaften Chemie Analytische Chemie
Naturwissenschaften Physik / Astronomie Elektrodynamik
Technik
Schlagworte Biopolymere • Chemie • Chemistry • NMR Spectroscopy / MRI / Imaging • NMR-Spektroskopie / MRT / Bildgebende Verfahren
ISBN-10 1-118-58889-4 / 1118588894
ISBN-13 978-1-118-58889-5 / 9781118588895
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